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碳化硅元件在不同气氛下使用温度和表面负荷的控制

2011-3-27
Control of applied temperature and surface load fo Songshan silca heating elements under different atmosphere

气氛Atmosphere

炉温Furnace Temp(℃)

表面负荷SurfaceLoad(w/cm2)

对元件的影响Acting to the element

解决办法Solve way

氨Ammonia

1290

3.8

与sic 作用生成甲烷减少SiO2保护膜Acting on SiC to form thus decrease SiO2 protective film

露点激活

Active at dew point

Co2

1450

3.1

侵蚀碳化硅 Attack SIC

用石英管保protected by quartz tube

18%co

1500

4.0

无影响 NOaction

20%co

1370

3.8

吸咐碳粒影响SiO保护膜Aadsorbing Cgrains to act on SiO2 protective film

卤素

Halogen

704

3.8

侵蚀碳化硅减少SiO2保护膜Adsorbing Cgrains to act on SiO2 protective film

用石英管保护

protected by quartz tube

碳氨化合物

hydrocarbon

1310

3.1

吸附碳粒而致热污染,分解的碳沉积,易造成电器故障Adsorbing C grains causes hot pollution

送进充分的空气fill with enough air

Hydrogen

1290

3.1

与SiC作用反应生成甲烷减少SiO保护膜

Acting on SiC and decreasing SiO2 protective film

露点激活

Active at dew point

甲烷

Methane

1370

3.1

吸附碳粒而致热污染Adsorbing C grains causes hot pollution

N

1370

3.1

与SiC反应形成氨化硅绝缘层 Acting with SiC forms SiN insulating layer

Na

1310

3.8

侵蚀碳化硅 Attack SiC

用石英管保
protected by quartz tube

So2

1310

3.8

侵蚀碳化硅 Attack SiC

用石英管保护protected by quartz tube

真空

Vacuum

1204

3.8

氧Oxygen

1310

3.8

碳化硅被氧化SiC is oxided

水(不同含量)water(different contents)

1090-1370

3.1~3.6

与SiC作用生成硅的水化物Acting on SiC forms hydtate of Si


根据炉子的结构,气氛和温度正确的选择元件的表面负荷是达到最佳使用寿命的关键。下图示出了元件辐射在不受阻碍情况下的炉温、元件温度与表面负荷之间的关系。
  The key factor to the optimum servece life of the element is to select the surface load of the element correctly according to the furnace construction,atmosphere and temperature.Below figure shows the relation between fumace temperatures,element temperature and element surface load under the condition that the element radiation isn’t obstructed.

推荐的元件表面负荷Recommend surface load

炉温℃Furnace Temp

1100

1200

1300

1350

1400

1450

发热部表面负荷Surface load of hot zone(W/㎝2)

<17

<13

<9

<7

<5

<4

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